Peculiarities of obtaining 2-hydroxyethyl-1,3,4-trimethylcyclohex-3-encarboxylate

I. S. Kostiv1 kostiv.irina [at] gmail.com
G. O. Marshalok1
  1. National University “Lviv Polytechnic,” st. Bandery 12, Lviv, 79013 Ukraine
Abstract 

The process of diene cyclization of 2,3-dimethylbutadiene with 2-hydroxyethylmethacrylate was investigated. Effects of temperature, reaction duration, and ratio of reagents on the yield of 2-hydroxyethyl-1,3,4-trimethylcyclohex-3-encarboxylate was studied. Optimal conditions of passing the process were found. Kinetic regularities of 2-hydroxyethyl-1,3,4-trimethylcyclohex-3-encarboxylate obtaining has been investigated. On the basis of the obtained results the optimal conditions of the target product synthesis have been established.

Keywords 
''2
3-dimethylbuta-1
3-diene''
2-hydroxy-ethylmethacrylate
''2-hydroxyethyl-1
3
4-trimethylcyclohex-3-encarboxylat''
cycloaddition reaction
References 

 

 

 

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[4] Polyova I., Marshalok G., Fedevych M. et al. (June 25, 2011). UA Pat. 60501, MPK С 07 С 13/20.

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